Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent
PhSCF2TMS was utilized as a useful gem-difluoromethylene building block for the synthesis of gem-difluoromethylenated spiro-γ-butyrolactones. The radical cyclization of γ-alkenyl- γ-gem-difluoro(phenylsulfanyl)methyl-γ-butyrolactones provided gem-difluoromethylenated spiro-γ-butyrolactones. PhSCF2TM...
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| التنسيق: | مقال |
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2018
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| الوصول للمادة أونلاين: | https://repository.li.mahidol.ac.th/handle/123456789/31510 |
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th-mahidol.315102018-10-19T11:47:00Z Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent Adisak Chatupheeraphat Darunee Soorukram Chutima Kuhakarn Patoomratana Tuchinda Vichai Reutrakul Chaveng Pakawatchai Saowanit Saithong Manat Pohmakotr Mahidol University Prince of Songkla University Chemistry PhSCF2TMS was utilized as a useful gem-difluoromethylene building block for the synthesis of gem-difluoromethylenated spiro-γ-butyrolactones. The radical cyclization of γ-alkenyl- γ-gem-difluoro(phenylsulfanyl)methyl-γ-butyrolactones provided gem-difluoromethylenated spiro-γ-butyrolactones. PhSCF2TMS (TMS = trimethylsilyl) is utilized as a gem-difluoromethylenating agent for the synthesis of gem-difluoromethylenated spiro-γ-butyrolactones. Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. 2018-10-19T04:47:00Z 2018-10-19T04:47:00Z 2013-10-01 Article European Journal of Organic Chemistry. No.30 (2013), 6844-6858 10.1002/ejoc.201300998 10990690 1434193X 2-s2.0-84885597753 https://repository.li.mahidol.ac.th/handle/123456789/31510 Mahidol University SCOPUS https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84885597753&origin=inward |
| institution |
Mahidol University |
| building |
Mahidol University Library |
| continent |
Asia |
| country |
Thailand Thailand |
| content_provider |
Mahidol University Library |
| collection |
Mahidol University Institutional Repository |
| topic |
Chemistry |
| spellingShingle |
Chemistry Adisak Chatupheeraphat Darunee Soorukram Chutima Kuhakarn Patoomratana Tuchinda Vichai Reutrakul Chaveng Pakawatchai Saowanit Saithong Manat Pohmakotr Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent |
| description |
PhSCF2TMS was utilized as a useful gem-difluoromethylene building block for the synthesis of gem-difluoromethylenated spiro-γ-butyrolactones. The radical cyclization of γ-alkenyl- γ-gem-difluoro(phenylsulfanyl)methyl-γ-butyrolactones provided gem-difluoromethylenated spiro-γ-butyrolactones. PhSCF2TMS (TMS = trimethylsilyl) is utilized as a gem-difluoromethylenating agent for the synthesis of gem-difluoromethylenated spiro-γ-butyrolactones. Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. |
| author2 |
Mahidol University |
| author_facet |
Mahidol University Adisak Chatupheeraphat Darunee Soorukram Chutima Kuhakarn Patoomratana Tuchinda Vichai Reutrakul Chaveng Pakawatchai Saowanit Saithong Manat Pohmakotr |
| format |
Article |
| author |
Adisak Chatupheeraphat Darunee Soorukram Chutima Kuhakarn Patoomratana Tuchinda Vichai Reutrakul Chaveng Pakawatchai Saowanit Saithong Manat Pohmakotr |
| author_sort |
Adisak Chatupheeraphat |
| title |
Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent |
| title_short |
Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent |
| title_full |
Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent |
| title_fullStr |
Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent |
| title_full_unstemmed |
Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent |
| title_sort |
synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing phscf<inf>2</inf>si(ch<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent |
| publishDate |
2018 |
| url |
https://repository.li.mahidol.ac.th/handle/123456789/31510 |
| _version_ |
1763495717176868864 |